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Mass Spectrometric Protein Footprinting of Conformational Changes Induced by Chromatographic Surfaces
Title
Mass Spectrometric Protein Footprinting of Conformational Changes Induced by Chromatographic Surfaces
Author
Focke, Kimberly
Date Created
2022
Subjects--Topical
Analytical chemistry, Biochemistry
Description
Reversed-phase liquid chromatography (RPLC) of intact proteins induces conformational changes due to the denaturing effects of both the hydrophobic stationary phase and the high-organic mobile phase, which can lead to poor recovery and badly disto...
Synthesis and Reactivity of Benzodiazepine-Derived Heterocyclic Thiones and Selones
Title
Synthesis and Reactivity of Benzodiazepine-Derived Heterocyclic Thiones and Selones
Author
Clinkscales, Alexander
Date Created
2021
Subjects--Topical
Chemistry, Inorganic, Chemistry, Organic, Analytical chemistry
Description
This thesis outlines the synthesis, characterization and coordination chemistry of new N-heterocylic benzodiazepine thione (NHT) and selone (NHSe) ligands. This new family of ligands, SBzDzArE (Ar = Xy, Mes, Dipp; E = S, Se), contain various bulky...
Synthesis and Reactivity of N-Heterocyclic Chalcogenone Complexes of Copper and Silver
Title
Synthesis and Reactivity of N-Heterocyclic Chalcogenone Complexes of Copper and Silver
Author
Allen, Alexander
Date Created
2018
Subjects--Topical
Chemistry, Inorganic, Chemistry, Organic, Analytical chemistry
Description
This presentation outlines the synthesis and characterization of several unusual two-coordinate copper(I) and silver(I) complexes supported by bulky N-heterocyclic thione (NHT) and selone (NHSe) ligands. More specifically, copper(I) complexes of t...